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Microwave assisted synthesis of Jeffamine cored PAMAM dendrimers

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dc.contributor.authorErturk, Ali S.
dc.contributor.authorTulu, Metin
dc.contributor.authorBozdogan, Abdurrezzak E.
dc.contributor.authorParali, Tezcan
dc.date.accessioned2026-06-27T13:30:15Z
dc.date.issued2014
dc.description.abstractThis study reports the use of a new microwave assisted amidation method for the synthesis of Jeffamine cored poly (amidoamine) (PAMAM) dendrimers up to fourth generations. Reaction proceeding is monitored by attenuated total reflectance (ATR) without final purification. It was found that current method decreases the aminolysis time, and minimizes the excessive use of reagents and solvents. Synthesized dendrimers were purified by liquid-phase polymer-based retention (LPR) technique and characterized by H-1-NMR, C-13-NMR, EA, GPC and UV-VIS spectroscopy. (C) 2014 Elsevier Ltd. All rights reserved.en
dc.description.sponsorshipYildiz Technical University Scientific Research Projects Coordination Department [2011-01-02-KAP04, 2011-01-02-KAP05, 2011-01-02-KAP06, 2012-01-02-DOP05]
dc.description.sponsorshipEU [2010-1-TR1-LEO05-16728]
dc.description.urihttps://doi.org/10.1016/j.eurpolymj.2013.12.018
dc.identifier.doi10.1016/j.eurpolymj.2013.12.018
dc.identifier.eissn1873-1945
dc.identifier.endpage226
dc.identifier.issn0014-3057
dc.identifier.startpage218
dc.identifier.urihttps://hdl.handle.net/20.500.14981/53297
dc.identifier.volume52
dc.identifier.wos000332436100021
dc.language.isoeng
dc.publisherPERGAMON-ELSEVIER SCIENCE LTD
dc.relation.ispartofEUROPEAN POLYMER JOURNAL
dc.subjectAmidation
dc.subjectDendrimers
dc.subjectLiquid phase polymer retention (LPR)
dc.subjectMicrowave chemistry (MW)
dc.subjectPOLY(AMIDOAMINE) DENDRIMERS
dc.subjectORGANIC-SYNTHESIS
dc.subjectPOLYMER
dc.subjectCHEMISTRY
dc.subjectCARRIERS
dc.subjectSIZE
dc.subjectPolymer Science
dc.titleMicrowave assisted synthesis of Jeffamine cored PAMAM dendrimers
dc.typeArticle
dspace.entity.typePublication
local.import.sourceWOS

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