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Synthesis and Characterization of a Novel Conformation of 2,9,10-Tribromoanthracene-1,4-dione

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dc.contributor.authorAkar, Kiymet Berkil
dc.contributor.authorCakmak, Osman
dc.contributor.authorSahin, Ertan
dc.date.accessioned2026-06-27T13:23:29Z
dc.date.issued2013
dc.description.abstractSynthesis and X-ray analysis of single crystals of 2,9,10-tribromoanthracene-1,4-dione 4 has been described and its novel conformation is reported. Single crystals were grown by slow evaporation technique from toluene solution at -15 A degrees C. The compounds have been characterized by elemental analysis, FT-IR, Mass and NMR spectroscopy. The compound crystallizes in the triclinic space group P-1 with unit cell dimensions a = 7.6842(2), b = 9.4865(2), c = 19.9388(4) , alpha = 78.784(5), beta = 76.980(5), gamma = 67.834(4) ; V: 1,301.75(7) (3); Z = 2, R (1) = 0.0748, and wR (2) = 0.131.en
dc.description.sponsorshipGaziosmanpasa University Research Foundation [2006/13, 2009/09]
dc.description.sponsorshipScientific and Technological Research Council of Turkey (TUBITAK) [105T426]
dc.description.urihttps://doi.org/10.1007/s10870-013-0472-4
dc.identifier.doi10.1007/s10870-013-0472-4
dc.identifier.eissn1572-8854
dc.identifier.endpage684
dc.identifier.issn1074-1542
dc.identifier.issue12
dc.identifier.startpage677
dc.identifier.urihttps://hdl.handle.net/20.500.14981/52544
dc.identifier.volume43
dc.identifier.wos000327215300007
dc.language.isoeng
dc.publisherSPRINGER/PLENUM PUBLISHERS
dc.relation.ispartofJOURNAL OF CHEMICAL CRYSTALLOGRAPHY
dc.subject1,4-Anthraquinone
dc.subjectBromoanthraquinone
dc.subjectSingle crystals
dc.subjectX-ray diffraction
dc.subjectCrystallography
dc.subjectSpectroscopy
dc.titleSynthesis and Characterization of a Novel Conformation of 2,9,10-Tribromoanthracene-1,4-dione
dc.typeArticle
dspace.entity.typePublication
local.import.sourceWOS

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