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Effect of modifying agents on the hydrophobicity and yield of zinc borate synthesized by zinc oxide

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dc.contributor.authorAcarali, Nil Baran
dc.contributor.authorBardakci, Melek
dc.contributor.authorTugrul, Nurcan
dc.contributor.authorDerun, Emek Moroydor
dc.contributor.authorPiskin, Sabriye
dc.contributor.institutionauthorACARALI, Nil
dc.date.accessioned2026-06-27T13:19:47Z
dc.date.issued2013
dc.description.abstractThe aim of this study was to synthesize zinc borate using zinc oxide, reference boric acid, and reference zinc borate (reference ZB) as the seed, and to investigate the effects of modifying agents and reaction parameters on the hydrophobicity and yield, respectively. The reaction parameters include reaction time (1-5 h), reactant ratio (H3BO3/ZnO by mass: 2-5), seed ratio (seed crystal/(H3BO3+ZnO) by mass: 0-2wt%), reaction temperature (50-120A degrees C), cooling temperature (10-80A degrees C), and stirring rate (400-700 r/min); the modifying agents involve propylene glycol (PG, 0-6wt%), kerosene (1wt%-6wt%), and oleic acid (OA, 1wt%-6wt%) with solvents (isopropyl alcohol (IPA), ethanol, and methanol). The results of reaction yield obtained from either magnetically or mechanically stirred systems were compared. Zinc borate produced was characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and contact angle tests to identify the hydrophobicity. In conclusion, zinc borate is synthesized successfully under the optimized reaction conditions, and the different modifying agents with various solvents affect the hydrophobicity of zinc borate.en
dc.description.urihttps://doi.org/10.1007/s12613-013-0768-6
dc.identifier.doi10.1007/s12613-013-0768-6
dc.identifier.eissn1869-103X
dc.identifier.endpage581
dc.identifier.issn1674-4799
dc.identifier.issue6
dc.identifier.startpage574
dc.identifier.urihttps://hdl.handle.net/20.500.14981/51886
dc.identifier.volume20
dc.identifier.wos000320284800011
dc.language.isoeng
dc.publisherSPRINGER
dc.relation.ispartofINTERNATIONAL JOURNAL OF MINERALS METALLURGY AND MATERIALS
dc.subjectzinc borate
dc.subjectzinc oxide
dc.subjecthydrophobicity
dc.subjectyield
dc.subjectBORIC-ACID
dc.subjectHYDROTHERMAL SYNTHESIS
dc.subjectAQUEOUS-MEDIUM
dc.subject2ZNO-CENTER-DOT-3B(2)O(3)CENTER-DOT-3H(2)O
dc.subjectMaterials Science
dc.subjectMetallurgy & Metallurgical Engineering
dc.subjectMining & Mineral Processing
dc.titleEffect of modifying agents on the hydrophobicity and yield of zinc borate synthesized by zinc oxide
dc.typeArticle
dspace.entity.typePublication
local.import.sourceWOS

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